DETERMINATION OF REACTION ENTHALPIES OF MOISTURE-SENSITIVE MATERIALS UNDER INERT GAS ATMOSPHERE | The enthalpy measurement of mixing reactions during the synthesis of air-sensitive materials must be carried out under inert conditions and thus places special demands on the measurement setup. One example of moisture-sensitive materials are sulfide solid-state electrolytes, which may be used in future solid-state batteries (ASSBs). To make these materials economically attractive, Fraunhofer IFAM is researching the scale-up of the synthesis process. For the upscaling of the syntheses, reaction enthalpies are required, which must be measured in an inert gas atmosphere.
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